By Slater J.C.
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During produced whether Another if the thermal would ordinary interest, fine-grained were limited used. to qualitative A focused heating a certain degree of sample vaporization. was the occurrence experienced observa- source was the same com- of phase separation in these systems. Thus, by these glasses were not identical, expect the degree and morphology than Hence, it was glasses were of precisely feature in general, glass. process due to the rapid unmixing histories that, beand it was noted that the crystal- glass was more techniques complicating of larger Laz05-AlsOs-SiO?
AT, is the elevation in immisccibility temperature relative to the data reported for T, by Haller et al. * In the fourth column the IR absorbances at 3600 cm-’ for these glassesare listed. This wave number corresponds to the location of the major water absorption. Another water absorption band is centered about 2700 cm-‘. The last column lists the ratio of the maximum peak intensities of the 2700 cm-’ to the 3600 cm-’ absorption bands. It should be mentioned that the gel glasseswere fabricated using somewhat different melting histories, and the gels were subjected to different drying procedures.
Offen. 173, August4, 1983; assigned to Owens-Illinois, Inc. 46. E. , Appl. Opt. 18, 3133 (1979). 44. 2 Simulation of the Sol-Gel Process Stephen H. Garofalini Rutgers-The Ceramics Department State University of New Jersey Piscataway, New Jersey INTRODUCTION Sol-gel though processing ferent additives mechanisms jectured on these from the and kinetic between functions n-mer) are not fully of the alkyl in complexity acid monomer, This or reported the dynamics process in better technique of Si02 hydrated molecules detail, the and of molecular is being used to study the in- molecules, the mechanisms of these molecules of reac- into which O-O, describe of alkyl the pyrosilicic have been in sol-gel processing probably larger involves at the onset of polymerization, (R) in the simulations was not deemed H4Si04, in certain experiments,“2 are being used for this study for several reasons.